Catalyst Preparation: Science and Engineering
By John Regalbuto
Publisher: CRC
Number Of Pages: 488
Publication Date: 2006-12-26
Book Description:
Improving the effectiveness of catalysts is the best way to ensure cleaner, more efficient industrial processes for a wide range of applications. Catalyst Preparation: Science and Engineering explores the optimization of catalytic materials through traditional and novel methods of catalyst preparation, characterization, and monitoring on laboratory and industrial scales.
The book presents many key principles of heterogeneous catalyst preparation and the methods used to synthesize a catalyst with a particular composition and morphology. The first chapters examine the synthesis of bulk materials including amorphous and mesoporous oxide supports, heteropolyacids, and colloidal metals. Subsequent chapters focus on the syntheses of heterogeneous nanoscale materials, including those based on metal complexsubstrate interactions and those using non-interacting precursors via viscous drying. The final chapters concentrate on pretreatment, drying, and finishing effects before concluding with a prognosis on future applications involving catalyst preparation and the technological advances necessary for continued progress.
An ideal companion for scientists exploring the preparation of application-specific catalysts based on desired catalytic properties, Catalyst Preparation: Science and Engineering provides a balanced overview of important synthesis parameters to consider for good catalyst design.
http://mihd.net/3tmowc
http://rapidshare.com/files/67147251/Catalyst_Preparation_Science_and_Engineering_0849370884.rar
Concepts of Modern Catalysis and Kinetics
By I. Chorkendorff, J. W. Niemantsverdriet
Publisher: Wiley-VCH
Number Of Pages: 469
Publication Date: 2003-12-30
Book Description:
Until now, the literature has offered a rather limited approach to the use of fundamental kinetics and their application to catalytic reactions. Subsequently, this book spans the full range from fundamentals of kinetics and heterogeneous catalysis via modern experimental and theoretical results of model studies to their equivalent large-scale industrial production processes. The result is key knowledge for students at technical universities and professionals already working in industry.
http://mihd.net/6tij3x
http://rapidshare.com/files/13411725/CMCK.rar.html
Interfacial Catalysis
By Alexander G. Volkov
Publisher: CRC
Publication Date: 2002-12-12
Book Description:
A comprehensive volume on interfacial catalysis, this book includes contributions from an international group of specialists in chemistry, environmental science, informatics, physiology, nuclear energy, and physics. The editor has organized the material into the main topics of fundamental characteristics, phase transfer catalysis, reversed micelles, biological aspects, and interfacial photocatalysis. Individual topics include self-organized microheterogeneous structures, nanochemistry, interfacial catalysis in metal complexation, the role of water molecules in ion transfer at the oil/water interface, and ultrathin films in enhanced oil recovery.
http://rapidshare.com/files/3061455/IC.rar
http://mihd.net/avtlr8
New Frontiers in Asymmetric Catalysis
By Koichi Mikami, Mark Lautens
Publisher: Wiley-Interscience
Number Of Pages: 418
Publication Date: 2007-05-04
Book Description:
A compilation of recent advances and applications in asymmetric catalysis
The field of asymmetric catalysis has grown rapidly and plays a key role in drug discovery and pharmaceuticals. New Frontiers in Asymmetric Catalysis gives readers a fundamental understanding of the concepts and applications of asymmetric catalysis reactions and discusses the latest developments and findings. With contributions from preeminent scientists in their respective fields, it covers:
"Rational" ligand design, which is critically dependent on the reaction type (reduction, oxidation, and C-C bond formation)
Recent findings on activation of C-H bonds, C-C bonds, and small molecules (C=O, HCN, RN=C, and CO2) and the latest developments on C-C bond reorganization, such as metathesis
Advances in "chirally economical" non-linear phenomena, racemic catalysis, and autocatalysis
Some of the recent discoveries that have led to a renaissance in the field of organocatalysis, including the development of chiral Brönstead acids and Lewis acidic metals bearing the conjugate base of the Brönstead acids as the ligands and the chiral bi-functional acid/base catalysts
The book ends with a thought-provoking perspective on the future of asymmetric catalysis that addresses both the challenges and the unlimited potential in this burgeoning field. This is an authoritative, up-to-date reference for organic chemists in academia, government, and industries, including pharmaceuticals, biotech, fine chemicals, polymers, and agriculture. It is also an excellent textbook for graduate students studying advanced organic chemistry or chemical synthesis.
http://mihd.net/c6rl0n
Heterogeneous Catalysis in Organic Chemistry
By Gerard V. Smith, Ferenc Notheisz
Publisher: Academic Press
Number Of Pages:346
Publication Date: 1999-07-15
Book Description:
The features of this book which will be of special interest to academic organic chemists are the introduction (Chapter 1), which presents a short course on the concepts and language of heterogeneous catalysis, covers organic reaction mechanisms of hydrogenation (Chapter 2), hydrogenolysis (Chapter 4), and oxidation (Chapter 6), a presents problems and solutions specific for running heterogeneous catalytic organic reactions in solution. These materials can supplement advanced chemistry courses.
Most synthetic organic chemists use a variety of "protecting groups" which they attach to functional groups (reactive groups of atoms) while some reaction is being conducted on another part of the molecule. These protecting groups prevent reactions of the functional groups during other reactions and are removed later by a heterogeneous catalytic method called hydrogenolysis. One unique feature of this book, not found in other books on catalysis, is an exhaustive chapter (Chapter 4) on hydrogenolysis, which is dredged from the recent synthetic literature published by modern organic chemists. Academic organic chemists should find this chapter extremely useful and may wish to adopt the book as a supplement for advanced organic chemistry courses designed for seniors and for graduate students. It will also be useful for professors and their research groups engaged in synthetic organic chemistry.
Many academic organic chemists are not aware of recent advances in heterogeneous enantioselective catalysis (Chapter 3) or in selective low temperature, liquid phase heterogeneous catalytic oxidations by hydrogen peroxide (Chapter 6). These specialty topics are timely and may be new to academic organic chemists and can be used to supplement their advanced courses.
Several features of this book will also be of special interest to industrial chemists who are unfamiliar with heterogeneous catalysis. Many good organic chemists are hire by industry. They synthesize a new compound using standard organic synthetic techniques but are informed by their supervisor that they must convert some of their synthetic steps into heterogeneous catalytic steps. They may not have been exposed to heterogeneous catalysis and have few places to turn. This book offers them a crash course in heterogeneous catalysis as well as many examples of reactions and conditions with which they can start their search.
Those industrial organic chemists already familiar with heterogeneous catalysis will find this book useful as a reference to many examples in the recent literature. They will find recent surface science discoveries correlated with heterogeneous catalysis or organic reactions and mechanistic suggestions designed to stimulate innovative nontraditional thinking about organic reactions on surfaces.
http://rapidshare.com/files/33192862/ewrdf.rar
http://mihd.net/crqh48
http://rapidshare.com/files/39567903/59612.rar
Micellar Catalysis (Surfactant Science)
By Mohammad Niyaz Khan
Publisher: CRC
Number Of Pages: 482
Publication Date: 2006-08-24
Book Description:
Micelles are prevalent in naturally occurring and biological catalytic reactions. However, it is only in recent decades that scientists have developed kinetic models clarifying how micelle-mediated catalysis works at a molecular level. Written by a leading expert in the field, Micellar Catalysis is an in-depth examination of how micelles affect reaction mechanisms and reaction rates in organic and inorganic reactions. The book first discusses the structural and chemical properties of micelles and the role of thermodynamics, concentration, and additives in forming micelles. Demonstrating how intermolecular forces influence the reaction mechanisms, the author presents kinetic models for reactions catalyzed by normal micelles, as well as mixed micelles and metallomicelles. The book also compares various types of catalytic reactions with and without micelles to quantify their effect on reaction rates and rate constants. Using this information, it illustrates how micelles can modify reaction rates and improve catalytic efficiency, particularly for industrial processes. The final chapter explains the principles of kinetics used for data analysis. Focused on kinetic, chemical, and physical aspects of micelle-mediated reactions, this book offers clear insight into the complex mechanisms that occur in biological reactions. Micellar Catalysis is an essential source of reference for scientists involved in the research and development of micelles for industrial and biochemical applications.
http://rapidshare.com/files/52902394/Kha1574444905.rar
http://mihd.net/xjotha
Catalysis by Gold (Catalytic Science)
By Geoffrey C. Bond, Catherine Louis, David T. Thompson
Publisher: Imperial College Press
Number Of Pages: 366
Publication Date: 2006-09-15
http://rapidshare.com/files/71545875/1860Bond946585.rar
Catalysis and Electrocatalysis at Nanoparticle Surfaces
By Andrzej Wieckowski, Elena R. Savinova, Constantinos G. Vayenas
Publisher: CRC
Number Of Pages 970
Publication Date: 2003-02-19
Book Description:
Catalysis and Electrocatalysis at Nanoparticle Surfaces illustrates the latest developments in electrochemical nanotechnology, heterogeneous catalysis, surface science, and theoretical modeling. It describes the manipulation, characterization, control, and application of nanoparticles for enhanced catalytic activity and selectivity and presents a range of experimental and synthetic strategies for work in nanoscale surface science. Thisis a comprehensive source for physical, surface, and colloid chemists; materials scientists; interfacial chemists and electrochemists; electrochemical engineers; theoretical physicists; chemical engineers; and upper-level undergraduate and graduate students in these disciplines.
http://rapidshare.com/files/1793545/Catalysis_and_Electrocatalysis_at_Nanoparticle_Surfaces.pdf
http://mihd.net/myb8rg
Surface and Interfacial Organometallic Chemistry and Catalysis
By Christophe Copéret, Bruno Chaudret
Publisher: Springer
Number Of Pages: 292
Publication Date: 2005-12-19
Book Description:
Heterogeneous catalysis has been essential to the development of efficient chemical processes for more than a century, and this field has been traditionally part of the solid state chemistry and surface science communities. The design of better catalysts has raised the following questions: "what is the structure of the active sites?" and "how to control their nature?" The necessary need to develop more sustainable chemical processes and the success of homogeneous catalysis relying on molecular organometallic chemistry has led the community of molecular chemists to investigate the preparation of single-site heterogeneous catalysts. The authors discuss the molecular design, the preparation, the characterisation and the catalytic applications of well-defined oxides and metal particles. The readers will acquire a molecular understanding of heterogeneous catalysis, which will help them develop a critical view and which will attract them to study this fascinating field.
http://mihd.net/7udx3y
http://rapidshare.com/files/44531299/vol16_surface_and_interfacial_organometallic.rar
Late Transition Metal Polymerization Catalysis
By Bernhard Rieger, Lisa Saunders Baugh, Smita Kacker, Susanne Striegler
Publisher: Wiley-VCH
Number Of Pages: 345
Publication Date: 2003-04-11
Book Description:
Even some fifty years after their discovery, transition metals have lost none of their fascination. The use of complex compounds in these elements has not only revolutionized synthesis in the laboratory, but has also led to them playing an important role in many industrial applications. Each year, millions of tons of plastics are produced around the world and, by varying the ligands in the catalytically active compounds, the properties of the resulting polymers can even be tailored for use.
For this purpose, sandwich compounds from early transition metals have been common until now, but interest has focused increasingly on the late transition metals. In this book, the world's leading authors from research and industry discuss the latest developments in research into palladium, zinc, iron and nickel catalysis. In so doing, they systematically introduce readers to the basic principles and illustrate how these innovative catalysts can be effectively used for polymerizations. The result is an ideal reference work, invaluable for every organic chemist working in catalysis or polymer research.
http://rapidshare.com/files/10226209/LTMPC.rar.html
Asymmetric Catalysis In Organic Synthesis (Baker Lecture Series)
By Ryoji Noyori
Publisher: Wiley-Interscience
Number Of Pages: 400
Publication Date: 1994-01
Book Description:
Deals with basic principles of asymmetric catalysis focusing on its synthetic significance. Covers homogeneous asymmetric hydrogenation, asymmetric catalysis via chiral metal complexes, heterogeneous catalysis and non-organometallic catalysis. The collection of a range of stereoselective reactions illustrate various strategies and methodologies as well as their general utility.
http://mihd.net/6z4nx8
By John Regalbuto
Publisher: CRC
Number Of Pages: 488
Publication Date: 2006-12-26
Book Description:
Improving the effectiveness of catalysts is the best way to ensure cleaner, more efficient industrial processes for a wide range of applications. Catalyst Preparation: Science and Engineering explores the optimization of catalytic materials through traditional and novel methods of catalyst preparation, characterization, and monitoring on laboratory and industrial scales.
The book presents many key principles of heterogeneous catalyst preparation and the methods used to synthesize a catalyst with a particular composition and morphology. The first chapters examine the synthesis of bulk materials including amorphous and mesoporous oxide supports, heteropolyacids, and colloidal metals. Subsequent chapters focus on the syntheses of heterogeneous nanoscale materials, including those based on metal complexsubstrate interactions and those using non-interacting precursors via viscous drying. The final chapters concentrate on pretreatment, drying, and finishing effects before concluding with a prognosis on future applications involving catalyst preparation and the technological advances necessary for continued progress.
An ideal companion for scientists exploring the preparation of application-specific catalysts based on desired catalytic properties, Catalyst Preparation: Science and Engineering provides a balanced overview of important synthesis parameters to consider for good catalyst design.
http://mihd.net/3tmowc
http://rapidshare.com/files/67147251/Catalyst_Preparation_Science_and_Engineering_0849370884.rar
Concepts of Modern Catalysis and Kinetics
By I. Chorkendorff, J. W. Niemantsverdriet
Publisher: Wiley-VCH
Number Of Pages: 469
Publication Date: 2003-12-30
Book Description:
Until now, the literature has offered a rather limited approach to the use of fundamental kinetics and their application to catalytic reactions. Subsequently, this book spans the full range from fundamentals of kinetics and heterogeneous catalysis via modern experimental and theoretical results of model studies to their equivalent large-scale industrial production processes. The result is key knowledge for students at technical universities and professionals already working in industry.
http://mihd.net/6tij3x
http://rapidshare.com/files/13411725/CMCK.rar.html
Interfacial Catalysis
By Alexander G. Volkov
Publisher: CRC
Publication Date: 2002-12-12
Book Description:
A comprehensive volume on interfacial catalysis, this book includes contributions from an international group of specialists in chemistry, environmental science, informatics, physiology, nuclear energy, and physics. The editor has organized the material into the main topics of fundamental characteristics, phase transfer catalysis, reversed micelles, biological aspects, and interfacial photocatalysis. Individual topics include self-organized microheterogeneous structures, nanochemistry, interfacial catalysis in metal complexation, the role of water molecules in ion transfer at the oil/water interface, and ultrathin films in enhanced oil recovery.
http://rapidshare.com/files/3061455/IC.rar
http://mihd.net/avtlr8
New Frontiers in Asymmetric Catalysis
By Koichi Mikami, Mark Lautens
Publisher: Wiley-Interscience
Number Of Pages: 418
Publication Date: 2007-05-04
Book Description:
A compilation of recent advances and applications in asymmetric catalysis
The field of asymmetric catalysis has grown rapidly and plays a key role in drug discovery and pharmaceuticals. New Frontiers in Asymmetric Catalysis gives readers a fundamental understanding of the concepts and applications of asymmetric catalysis reactions and discusses the latest developments and findings. With contributions from preeminent scientists in their respective fields, it covers:
"Rational" ligand design, which is critically dependent on the reaction type (reduction, oxidation, and C-C bond formation)
Recent findings on activation of C-H bonds, C-C bonds, and small molecules (C=O, HCN, RN=C, and CO2) and the latest developments on C-C bond reorganization, such as metathesis
Advances in "chirally economical" non-linear phenomena, racemic catalysis, and autocatalysis
Some of the recent discoveries that have led to a renaissance in the field of organocatalysis, including the development of chiral Brönstead acids and Lewis acidic metals bearing the conjugate base of the Brönstead acids as the ligands and the chiral bi-functional acid/base catalysts
The book ends with a thought-provoking perspective on the future of asymmetric catalysis that addresses both the challenges and the unlimited potential in this burgeoning field. This is an authoritative, up-to-date reference for organic chemists in academia, government, and industries, including pharmaceuticals, biotech, fine chemicals, polymers, and agriculture. It is also an excellent textbook for graduate students studying advanced organic chemistry or chemical synthesis.
http://mihd.net/c6rl0n
Heterogeneous Catalysis in Organic Chemistry
By Gerard V. Smith, Ferenc Notheisz
Publisher: Academic Press
Number Of Pages:346
Publication Date: 1999-07-15
Book Description:
The features of this book which will be of special interest to academic organic chemists are the introduction (Chapter 1), which presents a short course on the concepts and language of heterogeneous catalysis, covers organic reaction mechanisms of hydrogenation (Chapter 2), hydrogenolysis (Chapter 4), and oxidation (Chapter 6), a presents problems and solutions specific for running heterogeneous catalytic organic reactions in solution. These materials can supplement advanced chemistry courses.
Most synthetic organic chemists use a variety of "protecting groups" which they attach to functional groups (reactive groups of atoms) while some reaction is being conducted on another part of the molecule. These protecting groups prevent reactions of the functional groups during other reactions and are removed later by a heterogeneous catalytic method called hydrogenolysis. One unique feature of this book, not found in other books on catalysis, is an exhaustive chapter (Chapter 4) on hydrogenolysis, which is dredged from the recent synthetic literature published by modern organic chemists. Academic organic chemists should find this chapter extremely useful and may wish to adopt the book as a supplement for advanced organic chemistry courses designed for seniors and for graduate students. It will also be useful for professors and their research groups engaged in synthetic organic chemistry.
Many academic organic chemists are not aware of recent advances in heterogeneous enantioselective catalysis (Chapter 3) or in selective low temperature, liquid phase heterogeneous catalytic oxidations by hydrogen peroxide (Chapter 6). These specialty topics are timely and may be new to academic organic chemists and can be used to supplement their advanced courses.
Several features of this book will also be of special interest to industrial chemists who are unfamiliar with heterogeneous catalysis. Many good organic chemists are hire by industry. They synthesize a new compound using standard organic synthetic techniques but are informed by their supervisor that they must convert some of their synthetic steps into heterogeneous catalytic steps. They may not have been exposed to heterogeneous catalysis and have few places to turn. This book offers them a crash course in heterogeneous catalysis as well as many examples of reactions and conditions with which they can start their search.
Those industrial organic chemists already familiar with heterogeneous catalysis will find this book useful as a reference to many examples in the recent literature. They will find recent surface science discoveries correlated with heterogeneous catalysis or organic reactions and mechanistic suggestions designed to stimulate innovative nontraditional thinking about organic reactions on surfaces.
http://rapidshare.com/files/33192862/ewrdf.rar
http://mihd.net/crqh48
http://rapidshare.com/files/39567903/59612.rar
Micellar Catalysis (Surfactant Science)
By Mohammad Niyaz Khan
Publisher: CRC
Number Of Pages: 482
Publication Date: 2006-08-24
Book Description:
Micelles are prevalent in naturally occurring and biological catalytic reactions. However, it is only in recent decades that scientists have developed kinetic models clarifying how micelle-mediated catalysis works at a molecular level. Written by a leading expert in the field, Micellar Catalysis is an in-depth examination of how micelles affect reaction mechanisms and reaction rates in organic and inorganic reactions. The book first discusses the structural and chemical properties of micelles and the role of thermodynamics, concentration, and additives in forming micelles. Demonstrating how intermolecular forces influence the reaction mechanisms, the author presents kinetic models for reactions catalyzed by normal micelles, as well as mixed micelles and metallomicelles. The book also compares various types of catalytic reactions with and without micelles to quantify their effect on reaction rates and rate constants. Using this information, it illustrates how micelles can modify reaction rates and improve catalytic efficiency, particularly for industrial processes. The final chapter explains the principles of kinetics used for data analysis. Focused on kinetic, chemical, and physical aspects of micelle-mediated reactions, this book offers clear insight into the complex mechanisms that occur in biological reactions. Micellar Catalysis is an essential source of reference for scientists involved in the research and development of micelles for industrial and biochemical applications.
http://rapidshare.com/files/52902394/Kha1574444905.rar
http://mihd.net/xjotha
Catalysis by Gold (Catalytic Science)
By Geoffrey C. Bond, Catherine Louis, David T. Thompson
Publisher: Imperial College Press
Number Of Pages: 366
Publication Date: 2006-09-15
http://rapidshare.com/files/71545875/1860Bond946585.rar
Catalysis and Electrocatalysis at Nanoparticle Surfaces
By Andrzej Wieckowski, Elena R. Savinova, Constantinos G. Vayenas
Publisher: CRC
Number Of Pages 970
Publication Date: 2003-02-19
Book Description:
Catalysis and Electrocatalysis at Nanoparticle Surfaces illustrates the latest developments in electrochemical nanotechnology, heterogeneous catalysis, surface science, and theoretical modeling. It describes the manipulation, characterization, control, and application of nanoparticles for enhanced catalytic activity and selectivity and presents a range of experimental and synthetic strategies for work in nanoscale surface science. Thisis a comprehensive source for physical, surface, and colloid chemists; materials scientists; interfacial chemists and electrochemists; electrochemical engineers; theoretical physicists; chemical engineers; and upper-level undergraduate and graduate students in these disciplines.
http://rapidshare.com/files/1793545/Catalysis_and_Electrocatalysis_at_Nanoparticle_Surfaces.pdf
http://mihd.net/myb8rg
Surface and Interfacial Organometallic Chemistry and Catalysis
By Christophe Copéret, Bruno Chaudret
Publisher: Springer
Number Of Pages: 292
Publication Date: 2005-12-19
Book Description:
Heterogeneous catalysis has been essential to the development of efficient chemical processes for more than a century, and this field has been traditionally part of the solid state chemistry and surface science communities. The design of better catalysts has raised the following questions: "what is the structure of the active sites?" and "how to control their nature?" The necessary need to develop more sustainable chemical processes and the success of homogeneous catalysis relying on molecular organometallic chemistry has led the community of molecular chemists to investigate the preparation of single-site heterogeneous catalysts. The authors discuss the molecular design, the preparation, the characterisation and the catalytic applications of well-defined oxides and metal particles. The readers will acquire a molecular understanding of heterogeneous catalysis, which will help them develop a critical view and which will attract them to study this fascinating field.
http://mihd.net/7udx3y
http://rapidshare.com/files/44531299/vol16_surface_and_interfacial_organometallic.rar
Late Transition Metal Polymerization Catalysis
By Bernhard Rieger, Lisa Saunders Baugh, Smita Kacker, Susanne Striegler
Publisher: Wiley-VCH
Number Of Pages: 345
Publication Date: 2003-04-11
Book Description:
Even some fifty years after their discovery, transition metals have lost none of their fascination. The use of complex compounds in these elements has not only revolutionized synthesis in the laboratory, but has also led to them playing an important role in many industrial applications. Each year, millions of tons of plastics are produced around the world and, by varying the ligands in the catalytically active compounds, the properties of the resulting polymers can even be tailored for use.
For this purpose, sandwich compounds from early transition metals have been common until now, but interest has focused increasingly on the late transition metals. In this book, the world's leading authors from research and industry discuss the latest developments in research into palladium, zinc, iron and nickel catalysis. In so doing, they systematically introduce readers to the basic principles and illustrate how these innovative catalysts can be effectively used for polymerizations. The result is an ideal reference work, invaluable for every organic chemist working in catalysis or polymer research.
http://rapidshare.com/files/10226209/LTMPC.rar.html
Asymmetric Catalysis In Organic Synthesis (Baker Lecture Series)
By Ryoji Noyori
Publisher: Wiley-Interscience
Number Of Pages: 400
Publication Date: 1994-01
Book Description:
Deals with basic principles of asymmetric catalysis focusing on its synthetic significance. Covers homogeneous asymmetric hydrogenation, asymmetric catalysis via chiral metal complexes, heterogeneous catalysis and non-organometallic catalysis. The collection of a range of stereoselective reactions illustrate various strategies and methodologies as well as their general utility.
http://mihd.net/6z4nx8
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