Handbook of Chemicals and Safety

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Safety Assessment for Chemical Processes by Jorg Steinbach

John Wiley & Sons | 1998-12-23 | ISBN: 352728852X | 305 pages | PDF | 13.8 Mb

This book combines the author's experience of 15 years of research in the field of chemical safety and 10 years in the chemical industry. It provides newcomers with an easy access to the field and helps practitioners in the chemical industry to answer all questions concerning their daily work with hazardous materials or potentially dangerous chemical plants. The investigation of risks, and preventive measures to be taken to minimize the probability of an accident, as well as its consequences are explained.

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Handbook of Industrial and Hazardous Wastes Treatment, Volume II (Advances in Industrial and Hazardous Wastes Treatment)

Handbook of Industrial and Hazardous Wastes Treatment, Volume II (Advances in Industrial and Hazardous Wastes Treatment).

By Lawrence K. Wang, Yung-Tse Hung, Nazih K. Shammas

• Publisher: CRC Press
• Number Of Pages: 1376
• Publication Date: 2009-11-04
• ISBN-10 / ASIN: 1420072196
• ISBN-13 / EAN: 9781420072198

Product Description:

Most industrial and hazardous waste management resources cover the major industries and provide conventional in-plant pollution control strategies. Until now however, no book or series of books has provided coverage that includes the latest developments in innovative and alternative environmental technology, design criteria, managerial decision methodologies, and regional and global environmental conservation. The new Handbook of Advanced Industrial and Hazardous Wastes Treatment—together with its predecessor, the Handbook of Industrial and Hazardous Wastes Treatment—forms a complete and up-to-date resource that contains all the necessary technical information on hazardous industrial waste treatment.

Providing in-depth coverage of treatment and management technologies in wide-ranging industries that readers simply won’t find anywhere else, this cutting-edge text addresses wastes in areas including metal finishing, food processing, milk production, coal mines, foundries, and chemical manufacturing. It covers basic and advanced principles and applications in contemporary hazardous and industrial waste treatment and explores new methods of clean production, waste minimization, and the treatment of landfills and underground storage tanks. Coverage includes the latest developments in legislation, regulations, soil remediation, brownfield site restoration, bioremediation, enzymatic processes, and much more.

Complete with numerous figures, tables, examples, and case histories, this book provides technical and economical information on how to develop a total environmental control program that can benefit both industry and local municipalities. This book combined with the Handbook of Industrial and Hazardous Wastes Treatment forms a resource that is comprehensive in scope and directly applicable to waste management problems in a broad range of industries.

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2006 International Fire Code: Softcover Version by International Code Council

2006 International Fire Code: Softcover Version by International Code Council.

Publisher: Cengage Learning | March 6, 2006 | ISBN: 1580012558 | Pages: 434 | PDF | 48.8 MB

The 2006 International Fire Code, coordinated with the 2006 International Building Code, references national standards to comprehensively address fire safety in new and existing buildings. It provides modern, up-to-date fire code, and addresses conditions hazardous to life and property from fire, explosion, handling or use of hazardous materials, and the use and occupancy of buildings and premises. Prescriptive- and performance- based approaches to fire prevention and fire protection systems are emphasized. Topics addressed include fire department access, fire hydrants, automatic sprinkler systems, fire alarm systems, hazardous materials storage and use, and fire safety requirements for new and existing buildings and premises.

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Isocyanates: Sampling, Analysis, and Health Effects

Isocyanates: Sampling, Analysis, and Health Effects (Astm Special Technical Publication// Stp)

By ASTM International

• Publisher: ASTM International
• Number Of Pages: 144
• Publication Date: 2002-02-01
• ISBN-10 / ASIN: 0803128797
• ISBN-13 / EAN: 9780803128798

Product Description:

STP 1408 examines the latest data and technology on isocyanates, and features topics ranging from sampling and analysis methods to health effects. Isocyanates are widely used in many industrial processes because of their high activity and affinity to many substances, which lead to polymerization, as well as the properties for the resulting polymers. They are used in the production of adhesives, elastomers, binders, flexible or rigid foams, paints, and lacquers. Because these products are used in a large number of synthesis and processing industries, many workers may be at risk of hazardous exposure. In addition, the various chemical and physical states of mixtures of isocyanate monomers and prepolymers make it difficult to document exposure-related toxicity through valid environmental sampling and analysis methods. Therefore it is of the utmost importance that the knowledge and tools necessary for the safe use of these products be made available to provide protection to the worker and the environment. 11 peer-reviewed papers cover: Isocyanate Determination in Atmospheres features new developments in sampling and analysis methods for workplace and environmental monitoring, including direct reading instrumentation, and how they relate to characterization of isocynate monomers and oligomers. Sampling Strategy and Control details case studies; global effects; interpretation of test results; control measures; and personal protective equipment designed to meet compliance. Health Effects covers toxicology; different routes of exposure, such as skin contact as well as inhalation; biological monitoring; surface contamination determination; evaluation of health effects; and the diagnostics used to detect exposure.

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Green Reaction Media in Organic Synthesis

Green Reaction Media in Organic Synthesis.

By Mikami Koichi

Publisher: Wiley-Blackwell

Number Of Pages: 200

Publication Date: 2005-11-18

ISBN-10 / ASIN: 140513402X

ISBN-13 / EAN: 9781405134026

Binding: Hardcover

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Product Description: Green, sustainable chemistry involves the designing of chemical processes with a view to reducing or even eliminating the use and production of hazardous materials. Recent endeavors have focused on limiting the use of organic solvents and replacing them with new, environmentally benign media. The chemical industry is interested in these cost-effective, alternative solvents and processes. This book provides a broad overview of the three most commonly used green reaction media. Directed at synthetic organic chemists working in academic and industrial laboratories, it will also serve as a textbook for graduate courses on green chemistry. Successful green reactions are considered, and experimental sections at the ends of the chapters provide important practical details, with illustrations of potential applications. Sufficient information is included to allow selection of the most appropriate medium. Extensively referenced, the volume offers a point of entry into the detailed literature.

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Resources and References: Hazardous Waste and Hazardous Materials Management

Resources and References: Hazardous Waste and Hazardous Materials Management.
By Donna S. Kocurek, Bayle Haber

• Publisher: William Andrew
• Number Of Pages: 303
• Publication Date: 1996-01-14
• ISBN-10 / ASIN: 0815513518
• ISBN-13 / EAN: 9780815513513

Product Description:

This guide book provides references and resources for the complex field of hazardous waste and hazardous materials management. The book is divided into general topics such as air quality, industrial wastewater, pollution prevention, and risk assessment under hazardous waste management and chemical hazards, emergency planning, and hazard communication under hazardous materials management. Each individual section includes a list of annotated bibliographies of the most recent books by major publishers as well as established, standard references. Following the annotated titles, are additional references of books and documents by publishers, technical associations, and governmental agencies (primarily the U.S. Environmental Protection Agency). In general, only references from 1986 onward are included since the technology and regulations affecting hazardous waste and materials are constantly evolving.

Additional resources included in the book are video tapes for training and instruction, information services and databases, libraries, agency contacts, technical journals, and a list of publishers and ordering information. This book will be a useful reference to professionals in the environmental field who need an extensive, but concise source of technical information and contacts.

The book will be a valuable addition to individual libraries and will fill a current reference void in university libraries, and technical libraries in industry and government. At present there are very few technical bibliographies in the field, and none has covered topics related to hazardous materials and hazardous waste as extensively as this book.

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Waste Treatment in the Process Industries

Waste Treatment in the Process Industries.

by: Lawrence K. Wang, Yung-Tse Hung, Howard H. Lo, Constantine Yapijakis

Publisher: CRC Press | 1 edition (31 Oct 2005) | ISBN: 084937233X | Pages: 648 | PDF | 8.9 MB

# Supplies a concise, sharply focused, and economical reference for waste management personnel concentrated in the process industries

# Details the latest developments, technologies, practices, and solutions for hazardous waste treatment and disposal

# Includes chapters on bioassay, implementing industrial ecology, and applications of biotechnology to waste treatment

# Features coverage of the major industrial process plants or installations that have significant effects on the environment

Increasing demand on industrial capacity has, as an unintended consequence, produced an accompanying increase in harmful and hazardous wastes. Derived from the second edition of the popular Handbook of Industrial and Hazardous Wastes Treatment, Waste Treatment in the Process Industries outlines the fundamentals and latest developments in waste treatment in various process industries, such as pharmaceuticals, textiles, petroleum, soap, detergent, phosphate, paper, pulp, pesticides, rubber, and power. Comprehensive in scope, it provides information that is directly applicable to daily waste management problems throughout the industry.

The book contains in-depth discussions of environmental pollution sources, waste characteristics, control technologies, management strategies, facility innovations, process alternatives, costs, case histories, effluent standards, and future trends for the process industry. It includes extensive bibliographies for each type of industrial process waste treatment or practice, invaluable information to anyone who needs to trace, follow, duplicate, or improve on a specific process waste treatment practice.

A quick scan of the chapters and contributors reveals the depth and breadth of the book's coverage. It provides technical and economical information on how to develop the most feasible total environmental control program that can benefit both process industry and local municipalities.

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Synthesis of Tamiflu

Synthesis of Tamiflu.

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Oseltamivir (INN) (pronounced /ɒsəlˈtæmɨvɪr/) is an antiviral drug that is used in the treatment and prophylaxis of both Influenzavirus A and Influenzavirus B. Like zanamivir, oseltamivir is a neuraminidase inhibitor. It acts as a transition-state analogue inhibitor of influenza neuraminidase, preventing progeny virions from emerging from infected cells.

Oseltamivir was the first orally active neuraminidase inhibitor commercially developed. It is a prodrug, which is hydrolysed hepatically to the active metabolite, the free carboxylate of oseltamivir (GS4071). It was developed by Gilead Sciences and is currently marketed by Hoffmann-La Roche (Roche) under the trade name Tamiflu. In Japan, it is marketed by Chugai Pharmaceutical Co., which is more than 50% owned by Roche. Oseltamivir is generally available by prescription only.

Roche estimates that 50 million people have been treated with oseltamivir. The majority of these have been in Japan, where an estimated 35 million have been treated.

With increasing fears about the potential for a new influenza pandemic, oseltamivir has received substantial media attention. Governments, corporations, and even some private individuals are stockpiling the drug. Production is currently sufficient to meet the demand for seasonal influenza and for government stockpiling. It is possible that shortages could recur in the event of an actual influenza pandemic.

There are some methods for synthesis:

Karpf / Trussardi synthesis

The current production method includes two reaction steps with potentially hazardous azides. A reported azide-free Roche synthesis of tamiflu is summarised graphically below

The synthesis commences from naturally available (−)-shikimic acid. The 3,4-pentylidene acetal mesylate is prepared in three steps: esterification with ethanol and thionyl chloride; ketalization with p-toluenesulfonic acid and 3-pentanone; and mesylation with triethylamine and methanesulfonyl chloride. Reductive opening of the ketal under modified Hunter conditions[5] in dichloromethane yields an inseparable mixture of isomeric mesylates. The corresponding epoxide is formed under basic conditions with potassium bicarbonate. Using the inexpensive Lewis acid magnesium bromide diethyl etherate (commonly prepared fresh by the addition of magnesium turnings to 1,2-dibromoethane in benzene:diethyl ether), the epoxide is opened with allyl amine to yield the corresponding 1,2-amino alcohol. The water-immiscible solvents methyl tert-butyl ether and acetonitrile are used to simplify the workup procedure, which involved stirring with 1 M aqueous ammonium sulfate. Reduction on palladium, promoted by ethanolamine, followed by acidic workup yielded the deprotected 1,2-aminoalcohol. The aminoalcohol was converted directly to the corresponding allyl-diamine in an interesting cascade sequence that commences with the unselective imination of benzaldehyde with azeotropic water removal in methyl tert-butyl ether. Mesylation, followed by removal of the solid byproduct triethylamine hydrochloride, results in an intermediate that was poised to undergo aziridination upon transimination with another equivalent of allylamine. With the librated methanesulfonic acid, the aziridine opens cleanly to yield a diamine that immediately undergoes a second transimination. Acidic hydrolysis then removed the imine. Selective acylation with acetic anhydride (under buffered conditions, the 5-amino group is protonated owing to a considerable difference in pKa, 4.2 vs 7.9, preventing acetylation) yields the desired N-acetylated product in crystalline form upon extractive workup. Finally, deallylation as above, yielded the freebase of oseltamivir, which was converted to the desired oseltamivir phosphate by treatment with phosphoric acid. The final product is obtained in high purity (99.7%) and an overall yield of 17-22% from (−)-shikimic acid. It is noted that the synthesis avoids the use of potentially explosive azide reagents and intermediates; however, the synthesis actually used by Roche uses azides. Roche has other routes to oseltamivir that do not involve the use of (−)-shikimic acid as a chiral pool starting material, such as a Diels-Alder route involving furan and ethyl acrylate or an isophthalic acid route, which involves catalytic hydrogenation and enzymatic desymmetrization.

Corey synthesis

In 2006 the group of E.J. Corey published a novel route bypassing shikimic acid starting from butadiene and acrylic acid [6]. The inventors chose not to patent this procedure which is described below.

Butadiene 1 reacts in an asymmetric Diels-Alder reaction with the esterfication product of acrylic acid and 2,2,2-Trifluoroethanol 2 catalysed by the CBS catalyst. The ester 3 is converted into an amide in 4 by reaction with ammonia and the next step to lactam 5 is an iodolactamization with iodine initiated by trimethylsilyltriflate. The amide group is fitted with a BOC protective group by reaction with Boc anhydride in 6 and the iodine substituent is removed in an elimination reaction with DBU to the alkene 7. Bromine is introduced in 8 by an allylic bromination with NBS and the amide group is cleaved with ethanol and caesium carbonate accompanied by elimination of bromide to the diene ethyl ester 9. The newly formed double bond is functionalized with N-bromoacetamide 10 catalyzed with Tin(IV) bromide with complete control of stereochemistry. In the next step the bromine atom in 11 is displaced by the nitrogen atom in the amide group with the strong base KHMDS to the aziridine 12 which in turn is opened by reaction with 3-pentanol 13 to the ether 14. In the final step the BOC group is removed with phosphoric acid and the oseltamivir phosphate 15 is formed.

Shibasaki Synthesis

Also in 2006 the group of Masakatsu Shibasaki of the University of Tokyo published a synthesis again bypassing shikimic acid

Shibasaki Tamiflu Synthesis Part I

Shibasaki Tamiflu Synthesis Part II

An improved method published in 2007 starts with the enantioselective desymmetrization of aziridine 1 with trimethylsilyl azide (TMSN3) and a chiral catalyst to the azide 2. The amide group is protected as a BOC group with Boc anhydride and DMAP in 3 and iodolactamization with iodine and potassium carbonate first gives the unstable intermediate 4 and then stable cyclic carbamate 5 after elimination of hydrogen iodide with DBU.

The amide group is reprotected as BOC 6 and the azide group converted to the amide 7 by reductive acylation with thioacetic acid and 2,6-lutidine. Caesium carbonate accomplishes the hydrolysis of the carbamate group to the alcohol 8 which is subsequently oxidized to ketone 9 with Dess-Martin periodinane. Cyanophosphorylation with diethyl phosphorocyanidate (DEPC) modifies the ketone group to the cyanophosphate 10 paving the way for an intramolecular allylic rearrangement to unstable β-allyl phosphate 11 (toluene, sealed tube) which is hydrolyzed to alcohol 12 with ammonium chloride. This hydroxyl group has the wrong stereochemistry and is therefore inverted in a Mitsunobu reaction with p-nitrobenzoic acid followed by hydrolysis of the p-nitrobenzoate to 13.

A second Mitsunobu reaction then forms the aziridine 14 available for ring-opening reaction with 3-pentanol catalyzed by boron trifluoride to ether 15. In the final step the BOC group is removed (HCl) and phosphoric acid added to objective 16.

Fukuyama synthesis

Fukuyama Tamiflu Synthesis Part I

Fukuyama Tamiflu Synthesis Part II

Pyridine (1) is reduced with sodium borohydride in presence of benzyl chloroformate to the Bcz protected dihydropyridine 2. The asymmetric Diels-Alder reaction with acrolein 3 is carried out with the McMillan catalyst to the aldehyde 4 as the endo isomer which is oxidized to the carboxylic acid 5 with sodium chlorite, Monopotassium phosphate and 2-methyl-2-butene. Addition of bromine gives halolactonization product 6 and after replacement of the Bcz protective group by a BOC protective group in 7 (hydrogenolysis in the presence of Di-tert-butyl dicarbonate) a carbonyl group is introduced in intermediate 8 by catalytic Ruthenium(IV) oxide and sacrificial catalyst Sodium periodate. Addition of ammonia cleaves the ester group to form amide 9 the alcohol group of which is mesylated to compound 10. In the next step iodobenzene diacetate is added, converting the amide in a Hofmann rearrangement to the allyl carbamate 12 after capturing the intermediate isocyanate with allyl alcohol 11. On addition of sodium ethoxide in ethanol three reactions take place simultaneously: cleavage of the amide to form new an ethyl ester group, displacement of the mesyl group by newly formed BOC protected amine to an aziridine group and an elimination reaction forming the alkene group in 13 with liberation of HBr. In the final two steps the aziridine ring is opened by 3-pentanol 14 and boron trifluoride to aminoether 15 with the BOC group replaced by an acyl group and on removal of the other amine protecting group (Pd/C, Ph3P, and 1,3-dimethylbarbituric acid in ethanol) and addition of phosphoric acid oseltamivir 16 is obtained.

Ref:

1. Tamiflu

2. Total synthesis of Tamiflu

Introduction to Hazardous Waste Incineration

Introduction to Hazardous Waste Incineration.
By Joseph J. Santoleri, Joseph Reynolds, Louis Theodore

• Publisher: Wiley-Interscience
• Number Of Pages: 656
• Publication Date: 2000-10-24
• ISBN-10 / ASIN: 0471017906
• ISBN-13 / EAN: 9780471017905

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Herbert F. Bender and Philipp Eisenbarth,Hazardous Chemicals: Control and Regulation in the European Market

Herbert F. Bender and Philipp Eisenbarth,"Hazardous Chemicals: Control and Regulation in the European Market."
Wiley-VCH | March 30, 2007 | ISBN: 3527315411 | 409 pages | PDF | 7.04 mb

This practice-oriented guide covers the handling and use of hazardous chemicals at the workplace, including labelling and storage, transportation, occupational safety and proper registration with the European authorities. Current European Union legislation and directives are cited throughout the text, making this a valuable reference for companies and institutions both inside and outside of the EU common market.

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Dangerous Properties of Industrial and Consumer Chemicals

Dangerous Properties of Industrial and Consumer Chemicals.
Publisher: CRC | ISBN: 0824791835 | edition 1994 | CHM | 816 pages | 1,08 mb

This valuable resource provides detailed health and safety information on the hazardous and toxic properties of over 1,000 heavily used industrial and consumer chemicals. Lists chemicals both alphabetically and numerically according to their Chemical Abstract Service number permitting rapid access to specific data.

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Waste Treatment in the Process Industries

Waste Treatment in the Process Industries.
by: Lawrence K. Wang, Yung-Tse Hung, Howard H. Lo, Constantine Yapijakis
Publisher: CRC Press | 1 edition (31 Oct 2005) | ISBN: 084937233X | Pages: 648 | PDF | 8.9 MB

# Supplies a concise, sharply focused, and economical reference for waste management personnel concentrated in the process industries
# Details the latest developments, technologies, practices, and solutions for hazardous waste treatment and disposal
# Includes chapters on bioassay, implementing industrial ecology, and applications of biotechnology to waste treatment
# Features coverage of the major industrial process plants or installations that have significant effects on the environment

Increasing demand on industrial capacity has, as an unintended consequence, produced an accompanying increase in harmful and hazardous wastes. Derived from the second edition of the popular Handbook of Industrial and Hazardous Wastes Treatment, Waste Treatment in the Process Industries outlines the fundamentals and latest developments in waste treatment in various process industries, such as pharmaceuticals, textiles, petroleum, soap, detergent, phosphate, paper, pulp, pesticides, rubber, and power. Comprehensive in scope, it provides information that is directly applicable to daily waste management problems throughout the industry.

The book contains in-depth discussions of environmental pollution sources, waste characteristics, control technologies, management strategies, facility innovations, process alternatives, costs, case histories, effluent standards, and future trends for the process industry. It includes extensive bibliographies for each type of industrial process waste treatment or practice, invaluable information to anyone who needs to trace, follow, duplicate, or improve on a specific process waste treatment practice.

A quick scan of the chapters and contributors reveals the depth and breadth of the book's coverage. It provides technical and economical information on how to develop the most feasible total environmental control program that can benefit both process industry and local municipalities.

Table of Contents
IMPLEMENTATION OF INDUSTRIAL ECOLOGY FOR INDUSTRIAL HAZARDOUS WASTE MANAGEMENT, L.K. Wang and Donald B. A
BIOASSAY OF INDUSTRIAL AND HAZARDOUS WASTE POLLUTANTS, S.Y. Selivanovskaya, V.Z. Latypova, N.Y. Stepanova, and Y.-T.
IN-PLANT MANAGEMENT AND DISPOSAL OF INDUSTRIAL HAZARDOUS SUBSTANCES, L.K. Wang
APPLICATION OF BIOTECHNOLOGY FOR INDUSTRIAL WASTE TREATMENT, J.-H. Tay, S.T.-L. Tay, V. Ivanov, and Y.-T. Hung
TREATMENT OF PHARMACEUTICAL WASTES, S.K. Gupta, S.K. Gupta, and Y.-T. Hung
TREATMENT OF OILFIELD AND REFINERY WASTES, J.M. Wong and Y.-T. Hung
TREATMENT OF SOAP AND DETERGENT INDUSTRY WASTES, C. Yapijakis and L.K. Wang
TREATMENT OF TEXTILE WASTES, T. Bechtold and Y.T. Hung
TREATMENT OF PHOSPHATE INDUSTRY WASTES, C. Yapijakis and L.K. Wang
TREATMENT OF PULP AND PAPER MILL WASTES, S. Sumathi and Y.-T. Hung
TREATMENT OF PESTICIDE INDUSTRY WASTES, J.M. Wong
TREATMENT OF RUBBER INDUSTRY WASTES, J.R. Taricska, L.K. Wang, Y.-T. Hung, J.-H. Tay, and K.H. Li
TREATMENT OF POWER INDUSTRY WASTES, L.K. Wang.

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McGraw-Hill's I.V. Drug Handbook by Patricia Dwyer Schull

McGraw-Hill's I.V. Drug Handbook by Patricia Dwyer Schull.
Publisher: McGraw-Hill Professional | ISBN: 0071548637 | 2008 | PDF | 734 pages | 9.8 Mb rared

Product Description:

Administer I.V. medications knowledgeably, safely and confidently

Because there's no room for error, turn to McGraw-Hill's I.V. Drug Handbook. Featuring a strong focus on patient safety, administering and monitoring I.V. drugs, the Handbook delivers concise, practical guidance to help you carry out one of the most difficult tasks you face. Written by and for practicing nurses and pharmacists, the Handbook is reliable, comprehensive, and easy-to-use.

Everything you need for safe, successful I.V. drug administration:

* All-inclusive coverage of over 350 parenteral drugs with the latest warnings from the FDA
* Includes antibiotics, insulin, pain medications, emergency drugs -- and more coverage of chemotherapeutic agents with more supportive therapies than you'll find in any other text
* Provides the most comprehensive, specific, evidence-based guidelines on administering high-alert and hazardous drugs available anywhere
* Each drug monograph includes administration guidelines, covering preparation, dilution & compatibility, infusion rates, admixtures, supportive therapies and monitoring.
* Features a 32 page full-color patient safety insert describing measures for ensuring safe drug administration, including 6 pagea on inserting an I.V. catheter
* Uses distinctive icons to call your attention to “clinical alerts,” “life-threatening reactions,” “high-alert”, “hazardous” drugs, and more

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Hazardous Waste Handbook

Hazardous Waste Handbook
Butterworth-Heinemann; 3 edition | August 1, 2000 | ISBN: 0750671351 | 288 pages | PDF | 10 Mb

You get the feeling the authors have some genuine site experience. They note the everyday dangers of slips, mechanical injuries and drowning in lagoons, as well as those from the properties of the waste. Their advice is to be prepared for the activity you intend and the one you may be faced with. There are useful lists of the boring things you might need, such as rinse tubs for boots and plastic sheeting. Stainless steel is expensive material to use for a drum of waste, they say, so the contents are probably dangerous.
-Chemistry and Industry

'....offers a straightforward approach to protecting the workers who clean up the nation's hazardous waste sites and chemical spills. The book is designed to help supervisors and site inspectors find information quickly e.g. answering occupational health questions at the work site. The manual is comprehensive and covers such topics ranging from site characterization, air monitoring, personal protective equipment, decontamination, and site emergencies. Numerous health and safety checklists, hazardous chemical data sheets, and personal protective equipment recommendations are presented for field decisions. The book also provides practical information on protecting workers and details the costs of hazardous chemical waste cleanup.' - Industrial Environmental Management.

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Fire and Explosion Hazards Handbook of Industrial Chemicals by Tatyana A. Davletshina & Nicholas P. Cheremisinoff

Book Description
ISBN-0815514298
This handbook provides ready information on the fire and chemical reactivity of commonly used chemicals. Its purpose is to provide basic information important to the safe handling of chemicals and to help provide guidance in responding to a hazardous materials incident, in particular, incidents involving reactive chemicals and materials posing fire and explosion hazards.
The volume has been written for chemical handling specialists, first responders to hazardous materials incidents, and firefighters. The basic definition used for a hazard materials incident is any situation that may potentially lead to catastrophic fire or explosion, and or human exposure to a toxic chemical. This situation may result from a spill of a hazardous material, a leak from a storage vessel or shipping container, or the mixing of incompatible chemicals whereby a chemical reaction could occur resulting in the release of energy and generation of toxic and perhaps flammable by-products. The volume provides chemical specific information, providing the reader with rigorous information on the chemical of interest.
This book is a compendium of chemical specific fire and chemical reactivity data and information. More than 1000 chemicals have been researched and organized into a reference handbook for fire specialists, chemical handling specialists, and plant safety engineers. The specific information provided for chemicals includes the flammability characteristics, recommended fire extinguishing practices, fire extinguishing agents not to be used, behavior in fires, burning characteristics, chemical reactivity with regard to water and common materials, incompatible chemical mixtures, containment and neutralization methods for spills. This reference book has been designed as a data bank for the hazardous materials handling specialist and industrial safety managers dealing with large chemical inventories. It is intended to be used by fire and loss prevention specialists and as a basis for developing procedures for safe storing and handling of chemicals. The authors have included an extensive physical properties section on chemicals, with information most pertinent to fire response situations.

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books on corrosion for engineers and chemists

Encyclopedia of Corrosion Technology, Second Edition (Corrosion Technology)

P.E., Philip A. Schweitzer
Publisher: Marcel Dekker
Number Of Pages: 675
Publication Date: 2004-03-17

Description:
Clarifying types of corrosion and susceptible materials, defining metallurgical and related terminology, and outlining means to prevent and curb corrosion, the Encyclopedia of Corrosion Technology, Second Edition is an up-to-date, innovative presentation of all aspects of corrosion-arranging over 400 topics into 25 alphabetical entries for easy navigation. More explanatory than a data book and more user-friendly than a textbook, the Encyclopedia extends coverage into areas of application and factors impacting corrosion protection while furnishing some 300 tables to enhance its written entries.

http://rapidshare.com/files/108987875/EnCoTeCrc.rar
http://www.mediafire.com/?ckx0ckxegoe

Corrosion Science and Technology
David Talbot

Publisher: RC-Press

Number Of Pages: 406

Publication Date: 1997-12-28

Description:
Corrosion Science and Technology clarifies all the important background material and guides readers in its practical application. This text integrates the chemical, electrochemical, and metallurgical aspects of corrosion control for application in typical contemporary technologies with economical use of resources. The structures of water, oxides, and metals are examined and the characteristics of metals and alloys often specified for corrosion-resistant service are described. This book includes explanations of scientific principles and real world applications and case histories. Extensive information on additional corrosion-related literature is provided to guide readers to sources of more specific information.

http://rapidshare.com/files/117285699/0849382246.rar
http://mihd.net/k9ol87b/


Fundamentals of Metallic Corrosion: Atmospheric and Media Corrosion of Metals

P.E., Philip A. Schweitzer

Publisher: CRC

Number Of Pages: 752

Publication Date: 2006-12-22

Description:
Understanding corrosion is essential for selecting and maintaining equipment and structural components that will withstand environmental and process conditions effectively. Fundamentals of Metallic Corrosion: Atmospheric and Media Corrosion of Metals focuses on the mechanisms of corrosion as well as the action of various corrodents on metals and their alloys. The book is tailored to support specialists studying corrosion in metallic materials or using metallic materials. The first chapters describe different forms of metallic corrosion and the effects of atmospheric corrodents such as sulfur-, nitrogen- and chlorine-containing compounds. They also discuss the corrosive effects of weathering conditions and natural media including water, acids, salts, organics, and gases. The remaining chapters are divided into metal types and their alloys. They cover stainless, ferritic, and martensitic steels as well as nickel alloys, copper, copper alloys, aluminum, titanium, zinc, and lead. Each chapter examines the corrosion potential of the material and provides easy-to-use charts that specify their compatibility with selected corrodents. The book also compares the corrosion resistance of nonferrous metals and alloys.

http://rapidshare.com/files/67544180...0849382432.pdf

Analytical Methods In Corrosion Science and Engineering
Philippe Marcus, Florian B. Mansfeld

Publisher: CRC

Number Of Pages: 776

Publication Date: 2005-07-27

Description:
Damage from corrosion costs billions of dollars per year. Controlling corrosion requires a fundamental, in-depth understanding of the mechanisms and phenomena involved, and this understanding is best achieved through advanced analytical methods. The first book to treat both surface analytical and electrochemical techniques in a single reference, Analytical Methods in Corrosion Science and Engineering equips you with hands-on tools for solving corrosion problems and improving corrosion resistance. The book begins with the major surface analytical techniques, their principles, instrumentation, and the exact nature of the information derived from their measurements. Individual chapters are devoted to electron spectroscopy, ion analytical methods, nanoprobes, synchrotron methods, infrared spectroscopy, and glow discharge optical emission spectroscopy followed by recent developments in the application of radiotracer methods, nanoscratching, and nanoindentation. Coverage then moves to electrochemical techniques, beginning with an introduction to electrochemical instrumentation that reveals the requirements for accurate and meaningful measurements as well as potential errors and how to avoid them. The authors provide a thorough background of each technique and illustrate its use for a variety of corrosion systems, in many cases using examples of practical industrial applications. Contributed by a team of prominent experts from major universities and national research laboratories around the world, Analytical Methods in Corrosion Science and Engineering is the most comprehensive guide available for investigating surface corrosion.

http://rapidshare.com/files/67647531...0824759524.rar

Metallic Materials: Physical, Mechanical, and Corrosion Properties

P.E., Philip A. Schweitzer

Publisher: CRC

Number Of Pages: 712

Publication Date: 2003-01-07

Description:
Metallic Materials compares and contrasts the corrosion resistance of wrought stainless steel and high nickel alloys and explores recent advances in the production of exotic metals. It emphasizes the physical and mechanical properties, corrosion resistance, workability and cost of various metals. The author analyzes the physical and mechanical properties of metals, defines relevant terminology, describes the various forms of corrosion to which metals may be susceptible, examines wrought ferrous metals, alloys, and typical applications, and covers wrought nickel and high nickel alloys. This is a handy reference for the busy engineer and student in corrosion, materials, chemical, mechanical, civil, design, process, metallurgical, manufacturing, and industrial engineering.

http://rapidshare.com/files/112470275/0824747410.zip

http://www.filefactory.com/dlf/f/ac4...465655dcd5/j/0

Corrosion and Protection

Einar Bardal

Publisher: Springer

Number Of Pages 336

Publication Date: 2004-01-09

Description:
Corrosion is generally described as "an attack on a metallic material by reaction with it’s environment". The corrosion of metallic materials causes large economic losses and is a high risk for accidents. The cost of corrosion is great but it is possible to reduce this cost by a better employment of existing knowledge. Providing a thorough contribution to knowledge distribution, Bardal combines a description of practical corrosion processes and problems with a theoretical explanation of the various types and forms of corrosion, with particular attention to the interaction between description and theory. A well thought-out introduction to corrosion science, with excellent examples and useful tables of data. Exremley well illustrated with 167 diagrams and photographs. Contains extensive reference material utilising the latest international standards. Vital emphasis is placed on the connections between practical problems and basic scientific principles. Corrosion and Protection is an essential guide for engineering students, particularly those with a limited background in chemistry, such as mechanical, marine and civil engineering students and also provides a valuable reference source for practicing engineers.

http://rapidshare.com/files/88771280/CP1852337583.rar
http://www.zshare.net/download/714619962e63b8/

Corrosion Resistant Materials Handbook - Fourth Edition
D. J. De Renzo

Publisher: Noyes Publications

Number Of Pages: 965

Publication Date: 1986-04-01

Description:
Cut corrosion losses by choosing suitable commercially available corrosion resistant materials. The index of approximately 5,000 corrosive agents will assist the reader in finding the appropriate corrosion resistant material.

http://rapidshare.com/files/12500253...s_handbook.pdf
http://mihd.net/m85kjf

Corrosion Control Through Organic Coatings Amy Forsgren

Publisher: CRC

Number Of Pages: 184

Publication Date: 2006-04-25

Description:
Choosing the most suitable coatings for structures such as bridges and building supports can extend the service life of that structure significantly. Corrosion Control Through Organic Coatings discusses the most important variables in the testing, selection, and application of heavy-duty, organic corrosion-protection paints. The book addresses the maintenance and restoration of older infrastructure and industrial plant as well as coatings for new structures made from various types of steel. The author, Amy Forsgren, examines the mechanisms of aging and deterioration caused by ultraviolet light, condensation, temperature, and chemical reactions. She also provides a complete description of composition of anti-corrosive organic coatings, including pigments, binders, and additives. Ms. Forsgren suggests which corrosion tests provide the most useful information on coating performance and corrosion-protection. Several chapters review the advantages and disadvantages of of different surface preparation methods. In addition, the author considers the environmental impact of various coatings and recognizes health hazards posed by volatile organic compounds (VOC's), toxic or hazardous pigments such as lead, and silica dust exposure. She also offers recommendations for providing safe working environments for personnel handling surface preparation. Integrating engineering aspects and corrosion expertise with paint formulation knowledge and surface chemistry, Corrosion Control Through Organic Coatings provides unique coverage of the most advanced treatments for extending the life span of heavy-duty metal structures today.

http://mihd.net/dm763k/