Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials

Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials by: Kenneth J.D. MacKenzie, M.E. Smith
Publisher: Pergamon | April 1, 2002 | ISBN: 0080437877 | Pages: 740 | PDF | 33.72 MB

Techniques of solid state nuclear magnetic resonance (NMR) spectroscopy are constantly being extended to a more diverse range of materials, pressing into service an ever-expanding range of nuclides including some previously considered too intractable to provide usable results. At the same time, new developments in both hardware and software are being introduced and refined. This book covers the most important of these new developments. With sections addressed to non-specialist researchers (providing accessible answers to the most common questions about the theory and practice of NMR asked by novices) as well as a more specialised and up-to-date treatment of the most important areas of inorganic materials research to which NMR has application, this book should be useful to NMR users whatever their level of expertise and whatever inorganic materials they wish to study.

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Once againmy favourate book

Introduction to Modern Liquid Chromatography by: Lloyd R. Snyder Joseph J. Kirkland
Publisher: Wiley-Interscience | ISBN: 0471038229 | 2nd Edition edition (9 Jan 1980) | Pages: 881 | PDF | 8 MB

This Second Edition incorporates the latest developments in the practical application of LC. Covers the basic of LC, the six LC methods and their applications, and various specialized areas. Provides material for in-depth comprehension of how HPLC is performed, what the necessary materials are, and possible applications. Offers thorough treatment of such areas as quantitative and qualitative analysis by HPLC, preparative scale separations, gradient elution and column-switching, sample pretreatment and reaction detectors, automated systems for high-volume testing and/or samples requiring pretreatment, troubleshooting and sample artifacts, and selection and development of LC method for a particular applications.

Contents
1 Introduction, 1
2 Basic Concepts and Control of Separation, 15
3 Equipment, 83
4 Detectors, 125
5 The Column, 168
6 Solvents, 246
7 Bonded-Phase Chromatography, 269
8 Liquid-Liquid Chromatography, 323
9 Liquid-Solid Chromatography, 349
10 Ion-Exchange Chromatography, 410
11 Ion-Pair Chromatography, 453
12 Size-Exclusion Chromatography, 483
13 Quantitative and Trace Analysis, 541
14 Qualitative Analysis, 575
15 Preparative Liquid Chromatography, 615
16 Gradient Elution and Related Procedures, 662
17 Sample Pretreatment and Reaction Detectors, 720
18 Selecting and Developing One of the LC Methods, 752
19 Troubleshooting the Separation, 781.

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Spectral Methods and Their Applications

Ben-Yu Guo, Pen-Yu Kuo "Spectral Methods and Their Applications."
World Scientific Publishing Company | 1998-03 | ISBN: 9810233337 | 349 pages | PDF | 7,3 MB

This book presents the basic algorithms, the main theoretical results, and some applications of spectral methods. Particular attention is paid to the applications of spectral methods to nonlinear problems arising in fluid dynamics, quantum mechanics, weather prediction, heat conduction and other fields.

The book consists of three parts. The first part deals with orthogonal approximations in Sobolev spaces and the stability and convergence of approximations for nonlinear problems, as the mathematical foundation of spectral methods. In the second part, various spectral methods are described, with some applications. It includes Fourier spectral method, Legendre spectral method, Chebyshev spectral method, spectral penalty method, spectral vanishing viscosity method, spectral approximation of isolated solutions, multi-dimensional spectral method, spectral method for high-order equations, spectral-domain decomposition method and spectral multigrid method. The third part is devoted to some recent developments of spectral methods, such as mixed spectral methods, combined spectral methods and spectral methods on the surface.

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GMP/ISO Quality Audit Manual for Healthcare Manufacturers and Their Suppliers, Sixth Edition

GMP/ISO Quality Audit Manual for Healthcare Manufacturers and Their Suppliers, Sixth Edition.
Publisher: CRC | 452 pages | April 15, 2004 | ISBN: 0849318475 | PDF | 2 MB

Volume 2 of this set contains the full text of the FDA regulations, EC and IPEC guidelines, and ISO/BSI standards referenced in the checklists furnished in Volume I. The book is organized to provide fast access to the guidelines and regulations of interest.

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McGraw-Hill's I.V. Drug Handbook by Patricia Dwyer Schull

McGraw-Hill's I.V. Drug Handbook by Patricia Dwyer Schull.
Publisher: McGraw-Hill Professional | ISBN: 0071548637 | 2008 | PDF | 734 pages | 9.8 Mb rared

Product Description:

Administer I.V. medications knowledgeably, safely and confidently

Because there's no room for error, turn to McGraw-Hill's I.V. Drug Handbook. Featuring a strong focus on patient safety, administering and monitoring I.V. drugs, the Handbook delivers concise, practical guidance to help you carry out one of the most difficult tasks you face. Written by and for practicing nurses and pharmacists, the Handbook is reliable, comprehensive, and easy-to-use.

Everything you need for safe, successful I.V. drug administration:

* All-inclusive coverage of over 350 parenteral drugs with the latest warnings from the FDA
* Includes antibiotics, insulin, pain medications, emergency drugs -- and more coverage of chemotherapeutic agents with more supportive therapies than you'll find in any other text
* Provides the most comprehensive, specific, evidence-based guidelines on administering high-alert and hazardous drugs available anywhere
* Each drug monograph includes administration guidelines, covering preparation, dilution & compatibility, infusion rates, admixtures, supportive therapies and monitoring.
* Features a 32 page full-color patient safety insert describing measures for ensuring safe drug administration, including 6 pagea on inserting an I.V. catheter
* Uses distinctive icons to call your attention to “clinical alerts,” “life-threatening reactions,” “high-alert”, “hazardous” drugs, and more

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Analytical Method Development and Validation by Michael E. Swartz

Analytical Method Development and Validation by Michael E. Swartz (Editor), Ira S. Krull (Editor)
Publisher: CRC Press | 16 May 1997 | ISBN: 0824701151 | Pages: 96 | PDF | 4.2 MB

." . .a useful primer-type book covering validation of analytical methods. . . .recommended." ---Analyst "Stop and read this. . .book to understand a formal way to develop or to improve and validate your methods. . .. In answer to any query posed to you about your methods development technique, you could hand your well-worn copy of this small book to the questioner. There should be no further questions." ---INFORM

Describes analytical methods development, optimization and validation, and provides examples of successful methods development and validation in high-performance liquid chromatography (HPLC) areas. The text presents an overview of Food and Drug Administration (FDA)/International Conference on Harmonization (ICH) regulatory guidelines, compliance with validation requirements for regulatory agencies, and methods validation criteria stipulated by the US Pharmacopia, FDA and ICH.

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Terahertz Spectroscopy: Principles and Applications

Terahertz Spectroscopy: Principles and Applications.
Publisher: CRC | Pages: 360 | 2007-12-22 | ISBN 0849375258 | PDF | 13 MB

The development of new sources and methods in the terahertz spectral range has generated intense interest in terahertz spectroscopy and its application in an array of fields. Presenting state-of-the-art terahertz spectroscopic techniques, Terahertz Spectroscopy: Principles and Applications focuses on time-domain methods based on femtosecond laser sources and important recent applications in physics, materials science, chemistry, and biomedicine. Â

The first section of the book examines instrumentation and methods for terahertz spectroscopy. It provides a comprehensive treatment of time-domain terahertz spectroscopic measurements, including methods for the generation and detection of terahertz radiation, methods for determining optical constants from time-domain measurements, and the use of femtosecond time-resolved techniques. The last two sections explore a variety of applications of terahertz spectroscopy in physics, materials science, chemistry, and biomedicine.

With chapters contributed by leading experts in academia, industry, and research, this volume thoroughly discusses methods and applications, setting it apart from other recent books in this emerging terahertz field.

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Dean's Analytical Chemistry Handbook (2nd Edition.)

Dean's Analytical Chemistry Handbook (2nd Edition.)
McGraw Hill | 1114 Pages | 2004 | ISBN:0071410600 | PDF | 9 MB

This essential on-the-job resource for the analytical chemist has been revised and updated with 40% new material. Readers will find all the conventional wet and instrumental techniques in one exhaustive reference along with all the critical data needed to apply them. Worked examples, troubleshooting tips, and numerous tables and charts are provided for easy access to the data.
- The most up-to-date and complete guide to analytical chemistry available today
- NEW: 3 major chapters on Analysis of Indoor Air, Analysis of Pesticides, Analysis of Trace Metal.

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Chemistry of Spices

Chemistry of Spices .
Publisher: CABI | ISBN: 1845934059 | edition 2008 | PDF | 455 pages | 1,84 mb

Spices are high value, export-oriented crops used extensively in food and beverage flavourings, medicines, cosmetics and perfumes. Interest is growing however in the theoretical and practical aspects of the biosynthetic mechanisms of active components in spices as well as the relationship between the biological activity and chemical structure of these secondary metabolites. A wide variety of phenolic substances and amides derived from spices have been found to possess potent chemopreventive, anti-mutagenic, anti-oxidant and anti-carcinogenic properties.

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Hypervalent Iodine in Organic Synthesis

Hypervalent Iodine in Organic Synthesis (Best Synthetic Methods.)
by: A. Varvoglis & O. Meth-Cohn, Alan R. Katritzky, C. S. Rees
Publisher: Academic Press | December 16, 1996 | ISBN: 0127149759 | Pages: 223 | PDF | 8.82 MB

There will be no synthetic chemist who, after reading this book, will not try to include the valuable hypervalent iodine reagents in their synthetic plans.

The first organic compound of polyvalent iodine- (dichloroiodo)benzene, PhICI2-was prepared by C. Willgerodt, in 1885. However, it took some 50 years before its first reaction was announced and several more years for really useful synthetic applications. Similarly, the exceptional oxidizing properties of o-iodylbenzoic acid, known since 1893, were unveiled only in 1994. In the meantime, an explosive growth occurred in the field of polyvalent iodine, especially during the last 10 years. More than a dozen individual compounds have currently reached the status of reagent, and numerous members from various classes have emerged as valuable synthetic intermediates. The chemistry of hypervalent iodine compounds, as it is appropriate to name them, includes a wealth of important, sometimes unique, reactions, offering powerful synthetic tools. Today, their exclusion from the arsenal of the organic chemist is inexcusable.

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Organosulfur Chemistry in Asymmetric Synthesis

Organosulfur Chemistry in Asymmetric Synthesis by: Takeshi Toru, Carsten Bolm (Re Upload)
Publisher: Wiley-VCH | August 2008 | ISBN: 3527318542 | Pages: 432 | PDF | 4.37 MB

In this first book to gather the information on this hot topic otherwise widely spread throughout the literature, experienced editors and top international authors cover everything the reader needs—from the synthesis of chiral organosulfur compounds to applications and catalysis:

* Asymmetric synthesis of chiral sulfinates and sulfoxides
* Synthesis and use of chiral dithioacetal derivatives, ylids, chiral sulfoximines and sulfinamides
* Use of chiral sulfoxides as ligands in catalysis
* Asymmetric reactions of alpha-sulfenyl, alpha-sulfinyl and alpha-sulfonyl carbanions.

As a result, readers will be able to improve their own performance in asymmetric synthesis.

From the contents
Asymmetric synthesis of chiral sulfinates
Asymmetric synthesis of chiral sulfoxides
Asymmetric Transformations Mediated by Sulfinyl Groups
Synthesis and use of chiral dithioacetal derivatives
Synthesis and use of chiral ylids
Synthesis and use of chiral sulfoximines
Synthesis and use of chiral sulfinamides
Use of chiral sulfoxides as ligands in catalysis
Sulfones in asymmetric catalysis
Asymmetric reactions of alpha-sulfenyl carbanions
Asymmetric reactions of alpha-sulfinyl carbanions
Asymmetric reactions of alpha-sulfonyl carbanions
Theoretical studies of asymmetric reactions with sulfur reagents.

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This is a must see...............

Chicken a la Carte : Director: Ferdinand Dimadura | Genre: Drama | Produced In: 2005

Synopsis: This film is about the hunger and poverty brought about by Globalization. There are 10,000 people dying everyday due to hunger and malnutrition. This short film shows a forgotten portion of the society. The people who live on the refuse of men to survive. What is inspiring is the hope and spirituality that never left this people.

http://www.cultureunplugged.com/play/1081/Chicken-a-la-Carte

Stereochemistry (Tutorial Chemistry Texts)

Stereochemistry (Tutorial Chemistry Texts).

Royal Society of Chemistry | ISBN: 085404602X | 2002-01 | PDF | 170 pages | 14 Mb

Stereochemistry is defined as the study of the three-dimensional structure of molecules. Stereochemical considerations are important in both isomerism and studies of the mechanisms of chemical reactions. Implicit in a mechanism is the stereochemistry of the reaction: in other words, the relative three-dimensional orientation of the reacting particles at any time in the reaction. Concentrating on organic chemistry, early chapters deal mainly with definitions of terms such as chirality, enantiomers, diastereoisomers and racemisation, complete with suitable examples to illustrate key concepts. Use of a polarimeter and associated definitions are described, together with two different conventions D, L and R, S for specification of configuration. Chirality without a stereogenic centre, in molecules such as allenes for example, is also covered. The distinction between conformation and configuration is developed to include assignment of configurations to di-substituted cyclohexanes and to the decalins. The conventions E, Z and Re, Si are introduced for sp2 hybridised carbons as found in alkenes and carbonyl compounds. These aspects of stereochemistry are further explored through consideration of reactions such as SN2, elimination and addition reactions, ester hydrolyses, electrocyclic reactions and Diels-Alder cycloadditions.

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Molecular Chemistry of Sol-Gel Derived Nanomaterials

Robert Corriu, Nguyen Trong Anh, "Molecular Chemistry of Sol-Gel Derived Nanomaterials." 

Wiley | 2009 | ISBN: 0470721170 | 200 pages | PDF | 23,6 MB

Presenting the wide range of synthetic possibilities opened by sol-gel processes in the field of organic-inorganic materials, Molecular Chemistry of Sol-Gel Derived Nanomaterials discusses the state of the art in the synthesis of the various nanomaterials. The text includes examples of applications, including photoluminescent nanocomposites, grafted nanomaterials for selective separations of ions or isotopes, for cascade syntheses, chelation of transition metals and lanthanides by lamellar structured nanomaterials, and immobilized enzymes on mesoporous nanomaterials. This indispensable text for graduate students, engineers, and scientists concludes with a look toward future developments. 

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Zinc Oxide: Fundamentals, Materials and Device Technology

Hadis Morkoç, Ümit Özgür, "Zinc Oxide: Fundamentals, Materials and Device Technology." 

Wiley-VCH | 2009 | ISBN: 3527408134 | 488 pages | PDF | 8 MB

This reference covers the wide and rapidly growing field of biocatalysis. It combines complementary expertise from such areas as microbiology, enzymology, molecular biology structural biology and organic chemistry, thus highlighting the interdisciplinary nature of the subject. 

With its special focus on progress and new developments towards environmentally beneficial reactions with high levels of selectivity for the production of key compound classes, this book will enlighten both chemists and biologists as to the advances and opportunities existing in enzyme catalysis. 

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Advanced Organic Chemistry: Reactions, Mechanisms, and Structure

Advanced Organic Chemistry: Reactions, Mechanisms, and Structure. 

John Wiley & Sons; 4th edition | July 1, 1992 | ISBN: 0471601802 | 1495 pages | PDF | 94 Mb

Covering virtually every useful chemical reaction, this revised reference work discusses scope, limitation and mechanism. The text is organized by reaction type in order to facilitate ease of use. It contains over 10,000 references. 

"...the book remains tremendous value for money...more pages per buck than most other texts...so it will remain a firm favourite as a general organic text and an easy-to-use 1-volume reference...will undoubtedly appear in all organic chemistry libraries and probably on many chemists personal bookshelves too." (Organic Process Research & Development Journal, Vol. 5, No. 6, November 2001) 

"...tremendous value for money...so it will remain a firm favourite as a general organic text and an easy-to-use 1-volume reference..." -- Organic Process Research & Development Journal, Vol. 5, No. 6, November 2001 --This text refers to an out of print or unavailable edition of this title. 

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Introduction to Flat Panel Displays

Jiun-Haw Lee, David N. Liu, Shin-Tson Wu, "Introduction to Flat Panel Displays (Wiley Series in Display Technology)" 

Wiley | 2009 | ISBN: 0470516933 | 280 pages | PDF | 6 MB

Flat Panel Displays (FPDs) are a frequent feature in our daily lives, used in mobile phones, laptop computers, desktop computer monitors and TVs. Several display technologies have been developed for FPDs, such as liquid crystal display (LCD), plasma display panel (PDP), light emitting diode (LED), organic light emitting device (OLED) and field emission display (FED). 

Introduction to Flat Panel Displays describes the fundamental sciences behind each display technology: LCD, PDP, LED, OLED and FED including carbon nanotubes. It contains a comparative analysis of the different display technologies in which detailed overviews of each technology are linked together so as to provide a comprehensive reference for students and display engineers, alike. Solved problems as well as homework problems are provided in each chapter to help consolidate students’ reading, as well as solutions hosted on an accompanying website. 

Features include: 

the classifications and specifications of display technologies as guidelines for developing a display and judging their performances; 

principles for designing color displays with good color saturation and wide color gamut; 

basic operating principles of thin-film transistors (TFTs) and their applications to state-of-the-art TFT-LCD and TFT-OLED; 

an overview of FED fundamentals comprising the physics of field emission, as well as FED structure and display mechanism. 

Senior undergraduate and graduate students taking courses in engineering, physics and chemistry will benefit from the systematic approach used throughout the book, which will help to prepare students for entry into a display profession. Display engineers, research scientists and technicians working on the development of flat panel display technology will also find this book an invaluable resource. Comparisons of the strengths and weaknesses of each of the display technologies will help professionals to decide which to use for their applications. 

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A New Unifying Biparametric Nomenclature that Spans all of Chemistry

A New Unifying Biparametric Nomenclature that Spans all of Chemistry by: Seymour Elk (Author)
Publisher: Elsevier Science | June 3, 2004 | ISBN: 0444516859 | Pages: 324 | PDF | 10.24 MB

As a byproduct of historical development, there are different, unrelated systems of nomenclature for "inorganic chemistry", "organic chemistry", "polymer chemistry", "natural products chemistry", etc. With each new discovery in the laboratory, as well as each new theoretical proposal for a chemical, the lines that traditionally have separated these "distinct" subsets of matter continually grow more blurred. This lack of uniformity in characterizing and naming chemicals increases the communication difficulties between differently trained chemists, as well as other scientists, and greatly impedes progress. With the set of known chemicals numbering over 42,000,000 (in Chemical Abstracts' data base) and continually growing (about 2,000 new additions every day), the desirability for a unified system for naming all chemicals simultaneously grows. Moreover, in order to meet the requirements of disparate groups of scientists, and of society in general, the name assigned to a given chemical should, not only uniquely describe that substance, but also should be a part of a readily recognizable order for the entire field. For these purposes, a topology-based "bi-parametric" system of nomenclature is herein proposed.

- In this book, a new nomenclature system is proposed

- The new nomenclature is applicable to a three dimensional world, and is internally consistent

- This nomenclature unifies ALL branches of chemistry, removing the need for various presently existing sets of rules.

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Mass Spectrometry: A Foundation Course

Mass Spectrometry: A Foundation Course By K. Downard 

Publisher: Royal Society of Chemistry | 21-09-2004 | ISBN: 0854046097 | 210 pages | 13.4 Mb

Mass Spectrometry: A Foundation Course is a textbook covering the field of mass spectrometry across the chemical, physical, biological, medical and environmental sciences. Sufficient depth is provided for the reader to appreciate the reasons behind and basis for particular experiments. It is uniquely and logically organised to enable the book to form the basis for a university course in mass spectrometry at the undergraduate or postgraduate level. This is achieved by combining specific core sections coupled to optional areas of study tailored to students of the chemical, physical, biological, medical and environmental sciences. Recommended course structures are provided in the front of the book. 

Dedicated chapters are included on: organic mass spectrometry; ion chemistry - to emphasise the role of mass spectrometry in fundamental chemistry and physics; biological mass spectrometry including proteomics; mass spectrometry in medicine, environmental and surface science and accelerator mass spectrometry, to emphasise the importance of these areas. Each chapter concludes with key references and additional recommended reading material, making the book an excellent springboard to further study. 

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